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For both procedures, the resulting deposits were analysed by STM scanning tunneling microscopy , ellipsometry and XPS X-ray photoelectron spectroscopy. Enter your mobile number or email address below and we’ll send you a link to download the free Kindle App. Shopbop Designer Fashion Brands. The first process consisted of depositing cluster 5 by spin coating on a gold surface. Enabled Amazon Best Sellers Rank: Amazon Drive Cloud storage from Amazon. ComiXology Thousands of Digital Comics.

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AmazonGlobal Ship Orders Internationally. If you want to subscribe to this journal, see our rates You can purchase this item in Pay Per View: You can move this window by clicking on the headline. The owners of this website hereby guarantee to respect the legal confidentiality conditions, applicable in France, and not to disclose this data to third parties. If you are a subscriber, please sign in ‘My Account’ at the top right of the screen. The first process consisted of depositing cluster 5 by spin coating on a gold surface.

Two approaches have been used to anchor the heterometallic complex on the surface and generate monolayers.

xray palladium

The first process consisted of depositing cluster 5 by spin coating on a gold surface. The second was the immersion of a gold surface into a cluster solution. For both procedures, the resulting deposits were analysed by STM scanning tunneling microscopyellipsometry and XPS X-ray photoelectron spectroscopy.

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For the layers obtained by spin coating of a solution of cluster 5it was found that the cluster is not attached to the surface, but only deposited on it. In contrast, after immersion of a gold sray into a solution of 5 or 6anchoring of the complexes was clearly evidenced by XPS via the chemical shift of the S—2p binding energy toward lower binding energies.

xray palladium

Ces couches ont ensuite été analysées par STM Scanning tunneling pallaadiumpar ellipsométrie et par spectroscopie XPS X-ray photoelectron spectroscopy. Mixed-metal clusters, Self-assembly, Gold surfaces, Spectroscopy, Scanning tunneling microscopy, X-ray photoelectron spectroscopy.

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Access to the PDF text. Access to the full text of this article requires a subscription. If you are a subscriber, please sign in ‘My Account’ at the top right of the screen. If you want to subscribe to this journal, see our rates You can purchase this item in Pay Per View: Synthesis of functional heterometallic complexes and clusters containing molybdenum and palladium or platinum, sray self-assembly on gold surfaces and X-ray photoelectron spectroscopic studies.

Outline Masquer le plan. Preparation of the samples and analyses of the resulting layers.

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xray palladium

Results and discussion Synthesis and characterization of the heterometallic complexes. Experimental part Preparation of the gold substrates. Electronic supplementary information ESI available: CCDC reference numbers